Wiley, 2013. — 429 p.
This text will introduce you to analytical chemistry: the science of making quantitative measurements. Quantifying the individual components in a complex sample is an exercise in problem solving. An effective and efficient analyst will have expertise in
sampling, sample processing, and method validation;
the chemistry that can occur in a sample before and during analysis;
selecting an appropriate analytical method; and
proper record keeping, data analysis, and reporting of results.
I organize the discussion of the core principles of analytical chemistry into three parts:
analytical concepts such as calibration and uncertainty, sample preparation, classical (wet-chemical) methods, and molecular Uv/Vis spectroscopy.
Chemical equilibria involving acids, bases, complexes, and insoluble precipitates.
Electroanalytical methods, atomic and mass spectrometry, and chromatographic separations
Quantitative analysis using reactions that go to ‘‘COMPLETION’’
Making measurements
sample preparation, extractions, and chromatography
classical methods
molecular spectroscopy
reactions that do not go to ‘‘COMPLETION.’’ Equilibria in aqueous solutions
acid–BASE Equilibria and activity
buffer solutions and polyprotic acids
complexation and precipitation equilibria instrumental methods and analytical separations
electroanalytical chemistry
atomic spectrometry
analytical separations